Sudan 1 - 1687 Words

SYNTHESIS OF 1-PHENYLAZO-2-NAPHTHOL ABSTRACT Amines are compounds composed of nitrogen atoms bearing alkyl or aromatic compounds. Amines undergo interesting reactions, one of which is with the reaction with nitrous acid producing an azo dye. In this study, the experiment focused on synthesizing an observing the physical properties of Sudan-1. Sudan-1 is of the most common dyes found in waxes, oils and in some food ingredients specifically curry and chilli powder. Furthermore, this study aimed to understand the mechanism behind the synthesis of 1-phenylazo-2-naphtol. To be able to synthesize Sudan-1, preparation of phenyldiazonium chloride solution and ÃŽ ²- naphthol solution were done. Ingrain dyeing was also done in this experiment. The†¦show more content†¦The main reaction that occurred in the preparation of phenyldiazonium chloride solution was diazotization reaction. Diazotization is the reaction between a primary aromatic amine and nitrous acid at cold temperatures to diazonium salt compound.[2] Figure 1 below is the reaction exhibited by the phenyldiazonium chloride solution. As this experiment aimed to synthesize Sudan-1, two steps are done. The first step would be the reaction of a primary aromatic amine to produce a diazonium salt as seen in Figure 1. The second step, then, is the reaction of the diazonium salt with a strongly activated aromatic syste,l known as coupling reactions. Azo coupling is the reaction between a diazonium compound and aniline, phenol or other aromatic compound which produces an azo compound.[5] In this experiment ÃŽ ²-naphthol couples with the diazonium salt. Figure 2 below shows the coupling reaction of the benzene diazonium chloride with ÃŽ ²-naphthol and having the product of Sudan-1. Furthermore, figure 3 below is the summary of reactions of the synthesis of Sudan-1 in this experiment. Figure 3 Summary of Reactions in Synthesizing Sudan-1 Figure 3 Summary of Reactions in Synthesizing Sudan-1 In this experiment, a filter paper was used to undergo ingrain dyeing. Ingrain dyeing is an irreversible chemical reaction of the diazonium salt solution and the activating aromatic solution. An orange-red filter paper was produced after such procedure. The presence ofShow MoreRelatedPaper 2 - the Growth of Contemporary Christianity in Sudan1584 Words   |  7 PagesCHRISTIANITY IN SUDAN PRESENTED TO PROFESSOR MARK NICKENS FOR CHHI 302 – DO1 BY REV. JOSEPH T. 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